Correlation between hardness and SEM-EDS characterization of palm oil waste based biocoke

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Asri Gani, Erdiwansyah, Hera Desvita, Saisa, Mahidin, Rizalman Mamat, Zulhaini Sartika, Ratna Eko Sarjono

2024 Energy Geoscience Vol. 5 Issue 4 Article Cited by 9 SDG 12SDG 17 Quartile

Abstract

This research investigates the relationship between hardness and microstructure obtained through SEM-EDS analysis of palm oil waste-based biocoke. The mechanical qualities and chemical composition of biocoke are being studied concerning the influence of temperature conditions. The manufacturing temperature of biocoke may vary between 150 °C and 190 °C. Utilizing SEM-EDS, we were able to characterize the microstructure and analyze the elemental composition, while the Hardness Shore D approach was used for the most complex materials. These results highlight the possibility of optimizing production temperature to produce biocoke with better mechanical performance. They show a positive correlation between biocoke hardness and structured carbon content. At 150 °C and 180 °C, respectively, the EFB biocoke reached its maximum hardness level of 62 ± 5. At 190 °C, OPM biocoke generated a 60 ± 5 times greater hardness than that of OPM and OPF biocoke. The OPT biocoke sample had the highest porosity with a score of 0.86, or 85.76%. Furthermore, compared to EFB biocoke, OPM and OPF biocokes had a priority of 0.84 (84.20%) and 0.83 (83.48%), respectively. Biocoke hardness is a quality indicator of physical and chemical qualities; the vital link between biocoke hardness, structural features, and elemental composition supports this idea. © 2024 Sinopec Petroleum Exploration and Production Research Institute

Affiliations

Department of Chemical Engineering, Universitas Syiah Kuala, Banda Aceh, 23111, Indonesia; Faculty of Engineering, Universitas Serambi Mekkah, Banda Aceh, 23245, Indonesia; Research Center of Palm Oil and Coconut, Syiah Kuala University, Banda Aceh, 23111, Indonesia; Department of Environment Engineering, Universitas Serambi Mekkah, Banda Aceh, 23245, Indonesia; Research Center for Chemistry, National Research and Innovation Agency, B.J. Habibie Science and Techno Park, Serpong, Banten, South Tangerang, 15314, Indonesia; Department of Chemical Engineering, Universitas Serambi Mekkah, Banda Aceh, 23245, Indonesia; Centre for Automotive Engineering, Universiti Malaysia Pahang, Pekan, 26600, Malaysia; Department of Chemistry, Faculty of Mathematics and Science, Universitas Pendidikan Indonesia, Bandung, 40522, Indonesia

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